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ISSN Approved Journal No: 2455-2631 | Impact factor: 8.15 | ESTD Year: 2016
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Issue: June 2024

Volume 9 | Issue 6

Impact factor: 8.15

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Paper Title: Structural, Chemical Etching and Dissolution Studies on Gel Grown Urinary Crystals
Authors Name: Shailesh S Dongare
Unique Id: IJSDR2405090
Published In: Volume 9 Issue 5, May-2024
Abstract: Abstract: Most common urinary crystals (calculi) encountered are Brushite and Struvite. These crystals have been grown by single diffusion gel growth technique. Well defined kite shaped struvite crystals suitable for dislocation studies along with cluster shaped brushite crystals were obtained in about 25 days’ time. The structural studies show single phase formation with orthorhombic symmetry. On addition of barley extract from the top of the gel, the dissolution /denaturation of crystals occurs which in turn is seen to affect the XRD structure in solid state. The ‘a’ and ‘c’ lattice parameters are found to change with least effect on the ‘b’ parameter. Surface topography reveals clustered- spear shaped brushite crystals, which dissolve on treatment with barley extract. Perforations have been recorded on the well grown struvite crystals treated with barley extract. The crystals are water insoluble and etching studies show well defined, oriented etch pits on the habit face treated with sulphuric acid. Barley extract as well as acidic medium helps in dissolution/ denaturation of urinary calculi (crystals), as recorded in the study.
Keywords: key words - Sodium meta-silicate (SMS), Brushite (B), Struvite (S), XRD, Surface topography
Cite Article: "Structural, Chemical Etching and Dissolution Studies on Gel Grown Urinary Crystals ", International Journal of Science & Engineering Development Research (www.ijsdr.org), ISSN:2455-2631, Vol.9, Issue 5, page no.649 - 652, May-2024, Available :http://www.ijsdr.org/papers/IJSDR2405090.pdf
Downloads: 000342048
Publication Details: Published Paper ID: IJSDR2405090
Registration ID:211381
Published In: Volume 9 Issue 5, May-2024
DOI (Digital Object Identifier): https://doi.org/10.5281/zenodo.11213613
Page No: 649 - 652
Publisher: IJSDR | www.ijsdr.org
ISSN Number: 2455-2631

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